Products

HPLC Columns

TSKgel GMHhr-H

TSKgel GMHhr-H mixed bed columns are packed with rigid, multiple pore size, polymer beads that are blended to provide an extended linear calibration curve. Mixed bed columns are commonly used for unknown samples and for the analysis of polymers with a broad molecular weight distribution. These columns provide high resolution of polymers with molecular weights of less than 4 × 108 Da. 

The issue of shearing that occurs with the analysis of ultra-high molar mass polymers is overcome by the TSKgel GMHhr-H (S) column. The (S) is a reference to this shearing effect.

TSKgel GMHhr-H columns are shipped in THF, which can be exchanged for a wide variety of organic solvents.


 
P/NDescriptionParticle Size Housing MaterialID (mm)Length (cm)Price ($) 
0017360TSKgel GMHhr-H5Stainless Steel7.8302,442
          

Product Attributes

Matrix: polystyrene-divinylbenzene
Particle size (mean): 5 µm
Pore size (mean): mixed
Exclusion limit: 4.0 × 10Da
Max. temperature: 80° C

Polystyrene Calibration Curves

SEC_GMHhr-H-Calibration-Fig67rev.png

Columns: TSKgel HHR columns,
7.8 mm ID × 30 cm
Mobile phase: THF
Flow rate: 1.0 mL/min
Detection: UV @ 254 nm
Temperature: 25 °C
Samples: polystyrene standards

       

Shear Degradation Comparison

 

SEC_GMHhr-H-Fig71.png

Columns: A: TSKgel GMHHR, 5 µm,
7.8 mm ID × 30 cm
B: TSKgel GMHXL9 µm,
7.8 mm ID × 30 cm
C: TSKgel GMHHR-H (S),
13 µm, 7.8 mm ID × 30 cm

Mobile phase: THF
Flow rate: 1.0 mL/min
Detection: UV @ 254 nm
Temperature: 25 °C
Sample: polystyrene standard F2000
(2.06 × 107 Da) 20 µL (0.025%)
Code #DescriptionLiterature Type
AN075 Analysis of Renewable-Based Polymers using the EcoSEC GPC System Coupled to Multi-Angle Light ScatteringApplication Note
IM01 TSKgel Column Instruction ManualInstruction Manual
LCAT01D TSKgel U/HPLC Columns 2019 Product Guide -- SEC, H Series ColumnsProduct Catalog
SR083 Solvent-Compatible High Performance GPC Columns: TSKgel Hhr SeriesSeparation Report
P/NDescriptionParticle Size Housing MaterialID (mm)Length (cm)Price ($) 
0017369TSKgel G5000Hhr-G7000Hhr and GMHhr-M;-N;-H Guard Column for 7.8 mm ID columns5Stainless Steel64784