TSKgel GMHhr-H (S) HT

The TSKgel GMHhr-H (S) HT high temperature mixed bed column is packed with rigid 13 µm polymer beads and is for the analysis of organic-soluble polymers. This column is for applications up to 140 °C and is shipped in o-dichlorobenzene (ODCB), which can be exchanged for 1-chloronaphthalene and trichlorobenzene. The issue of shearing that occurs with the analysis of ultra-high molar mass polymers is overcome by the TSKgel GMHhr-H (S) HT column. The (S) is a reference to this shearing effect.

The TSKgel mixed bed columns are packed with particles of different pore sizes that are blended to provide an extended linear calibration curve. Mixed bed columns are used when a broad range of polymer molar masses is expected in the sample.

P/N	Description	Particle Size (µm)	Housing Material	ID (mm)	Length (cm)	Price ($)
0018393	TSKgel GMHhr-H (S) HT	13	Stainless Steel	7.8	30	3,059	Inquire

Product Attributes

Matrix:	polystyrene-divinylbenzene
Particle size (mean):	13 µm
Pore size (mean):	mixed
Exclusion limit:	4 × 10⁸Da
Max. temperature:	140 °C

Polystyrene Calibration Curves

Columns:	TSKgel G2000HHR(20) HT, 20 µm, 7.8 mm ID × 30 cm TSKgel GMHHR-H HT, 5 µm, 7.8 mm ID × 30 cm TSKgel GMHHR-H(S) HT, 13 µm, 7.8 mm ID × 30 cm TSKgel GMHHR-H(20) HT, 20 µm, 7.8 mm ID × 30 cm TSKgel GMHHR-H(30) HT, 30 µm, 7.8 mm ID × 30 cm
Mobile phase:	ODCB with 0.05% BHT
Flow rate:	1.0 mL/min
Detection:	RI (EcoSEC High Temperature GPC System)
Temperature:	135 °C
Injection vol.:	300 µL
Sample:	polystyrene

Comparison of Column Durability at 220 °C

GPC elution profile for a polymer before and after temperature cycling obtained using a TSKgel GMHHR-H (S) HT column (left) and a commercially available high temperature column (right)

Columns:	TSKgel GMHHR-H (S) HT, 13 µm, 7.8 mm ID × 30 cm Commercially available high temperature GPC column, 13 µm, 7.8 mm ID × 30 cm
Mobile phase:	1-chloronaphthalene
Flow rate:	1.0 mL/min
Detection:	RI
Temperature:	220 °C
Injection vol.:	220 µL
Samples:	synthetic polymer

Code #	Description	Literature Type
AN062	TSKgel High Temperature GPC Column Durability	Application Note
DS1240	TSKgel HT and HT2 (High Temperature) Products	Operating Conditions and Specifications
IM01	TSKgel Column Instruction Manual	Instruction Manual
LCAT01D	TSKgel U/HPLC Columns 2019 Product Guide -- SEC, H Series Columns	Product Catalog

P/N	Description	Particle Size (µm)	Housing Material	ID (mm)	Length (cm)	Price ($)
0018397	TSKgel GMHhr-H (S) HT Guard Column for 7.8 mm ID column	30	Stainless Steel	7.5	7.5	741

HPLC Columns

TSKgel GMHhr-H (S) HT

Product Attributes

Polystyrene Calibration Curves

Comparison of Column Durability at 220 °C