Separation of Triglycerides
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Columns: |
TSKgel ODS-100Z, 3 µm,
4.6 mm ID × 15 cm
|
Mobile phase: |
A: Acetonitrile
B: THF |
Gradient: |
0 min (20% B) 20 min (60% B)
22 min (60% B) 23 min (20% B)
28 min (20% B) |
Flow rate: |
1 mL/min |
Detection: |
ELSD: temp: 50 °C, Gain: 6, Nebulizer Gas: N2, Gas Pressure: 360 kPA |
Temperature: |
40 °C |
Injection vol.: |
10 µL |
Samples: |
1. tricaproin 2. tricaprylin
3. tricaprin 4. trilaurin
5. trimyristin 6. tripalmitin
7. tristearin 8. triolein
9. trilinolein |
Sample load: |
0.5 g/L each |
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