Separation of 16 Poly-aromatic Hydrocarbons
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Columns: |
TSKgel ODS-120A, 5 µm, 4.6 mm ID × 25 cm
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Gradient: |
40 min linear from 75% MeOH/25% H2O to 95% MeOH/5% H2O, 5 min hold |
Flow rate: |
1.2 mL/min
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Detection: |
UV @ 254 nm |
Temperature: |
40 °C |
Samples: |
5 mL mixture of:
1. naphthalene
2. acenaphthylene
3. acenaphthene
4. fluorene
5. phenanthrene
6. anthracene
7. fluoranthene
8. pyrene
9. benzo(a)anthracene
10. chrysene
11. benzo(b)fluoranthene
12. benzo(k)fluoroanthen
13. benzo(a)pyrene
14. dibenzo(a,h)anthracene
15. benzo(g,h,i)perylene
16. indeno(1,2,3-cd)pyrene |
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