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LenS3 MALS-V Dual Detector

The LenS3 MALS-V dual detector is a LenS3 MALS detector (allowing direct measurement of molecular weight and provides best-in-class sensitivity) equipped with an optional integrated viscometer. It offers a simple and compact solution for triple detection measurements when combined with a concentration detector (RI or UV). Just like with light scattering data, the SECview software includes seamless viscometry data acquisition and processing to get the most out of advanced detection GPC/SEC analyses.

A perfect complement to MALS for polymer analysis
The intrinsic viscosity (IV) of polymers reflects how dense and how flexible polymer chains are in dilute solutions. The lower the IV, the more compact the polymer is while rigid polymer chains show a higher IV than flexible random coils.

When combined with light scattering measurements, the MW and IV distributions provide a wealth of structural information
about polymers:

  • conformation (random coil, sphere, rod)
  • density of the backbone
  • presence of branching (number of branches, branching frequency)
  • hydrodynamic radius (Rh)
  • Mark-Houwink parameters

The viscometer also allows the determination of MW by universal column calibration for comparison with legacy methods or for special applications to polymers with unfavorable optical properties (e.g. weak scatterers, light absorption and fluorescence).


 
P/NDescriptionPrice
($)
 
0040200LenS3 MALS-V Dual Detector-


Specifications

Light scattering
Number of measurement angles 3
Position of the measurement angles LALS (10°)   RALS (90°)   HALS (170°)
Cell geometry proprietary conical flow path (single inlet, dual outlets)
Laser source type diode
Laser power 20 mW +/- 5
Laser wavelength 505 nm
Laser temperature control yes
Wetted material teflon, PEEK, glass, stainless steel
Maximum flow rate 2 mL/min
Inlet position front or side
Baseline noise (in THF @ 1 mL/min) < 1 mV
Baseline drift (in THF @ 1 mL/min) < 1 mV / 30 min
MW range < 200 to 107 Da
Rg range < 2 nm to > 50 nm (in progress)



Viscometer (optional)
Measurement principle 4-capillary differential bridge
Dynamic range 5 kPA
Linearity 0.1 % full scale
Baseline noise (in THF @ 1 mL/min) < 0.2 Pa
Baseline drift (in THF @ 1 mL/min) < 0.25 Pa / 60 min
Volume 23 µL per capillary
Maximum flow rate 4 mL/min in THF; 2 mL/min in water
Maximum pressure 200 kPA
Maximum detector backpressure at outlet 50 kPA
Wetted material Teflon, stainless steel, PEEK
Delay volume Small, Medium or Large



General
A/D board channels / resolution 8 channels / 24 bits
Acquisition rate 10 Hz
Dynamic range +/- 10 V
Analog inputs RI, UV and start signal
Connection to PC ethernet
Dimensions 36.5 (W) × 48.5 (D) × 13 (H) mm = 14.4" × 19.1" × 5.1"
Weight 176 kg = 37 lbs (LenS3 MALS-V)
Intellectual property PCT/US19/12090: Light Scattering Detectors and Sample Cells for the Same
PCT/US19/12095: Light Scattering Detectors and Methods for the Same
PCT/US2023/025136: Detector for Viscosity and Light Scattering and Methods for the Same

Code #DescriptionLiterature Type
AN145 Greener Solvent Alternatives in GPC/SEC and Light Scattering Analyses of PolymersApplication Note
BR11 A New Paradigm in Light Scattering Technology: Solution for advanced GPC/SEC detectionBrochure
TN001 Expanding the Boundaries of Light Scattering DetectionTechnical Note
WP001 Light Scattering for Determination of Molecular Weight and Radius of GyrationWhite Paper